NMR Services:


Varian 300 MHz


Proton NMR:

We use about 5-10 mg of sample which is dissolved in 0.6 ml of NMR Solvent.

C-13 NMR:

A higher concentration of 20-50 mg/0.6 ml is required for good S/N ratio. DMSO (39.51 ppm) is used externally for C-13 chemical shift calibration in D2O.


Data is stored in the computer system for at least two weeks. Older data files are permanently stored on the server. Data is made available by request via e-mail.


Full spectrum (10 to -.5 ppm H-1, or 200 to 0 ppm C-13), and expansions with integration and peak-picking are sent to you within 24 hours for routine analysis.

Mass Spec Services


Perkin Elmer PE-SCIEX API-150.

Detection range = 30 – 3000 amu.


We use 1 ug of sample to be dissolved in 1 ml of suitable solvent.




We offer reports by fax, mail, or e-mail for both positive and negative spectra. Our standard procedure scans 300-500 amu with molecular ion near the center of the spectrum.


NMR Analysis:

Routine Analysis

F-19 Analysis = $75 per Analysis

Long Experiment (Polymers, etc) = $65/hour

Mass: $35 Per Analysis

HPLC: $50 Per Analysis with two conditions

How to place an order:

How to use the Order form

  1. Our order form uses tables in Microsoft Word. Completing the form simply requires you to fill out the sections marked by an empty entry of a table. Just simply click on the empty table and type in the information. You can save the order form onto the computer for future use.
  2. For each desired test, you would fill out the necessary information in each respective section. For example, to run both NMR and Mass, you would fill out only the NMR and Mass sections
  3. Things we need to know for each test you would like conducted:
    • NMR: Please let us know the solvent and the type of test (H1, C13, etc)
    • Mass: Please indicate the molecular weight (M.W.) and range you would like scanned.
  4. Click the link below for the order form in Microsoft Word format. You can save it on your computer by right clicking on the link and then left clicking on save as.

Please give us a call or contact us by email for any other questions.